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Figure 13.25. Photo and thermal isomerization of azobenzene ligands in the photoresponsive aerogel. (a) As-prepared, (b) after UV irradiation of sample (a) for 40 min, (c) after room light exposure of sample (b) for 60 min, (d) after heating sample (b) to 1001C for 10 min.

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cis conformation in the as-prepared lm. Using a molar absorption coef cient (e) of 2.59 104 M 1 cm 1 for the trans isomer of TSUA, the concentration of the trans isomer in the lm was estimated to be 0.27, 0.22, 0.20, and 0.17 M for lm samples in Fig. 13.25d, a, c and b, respectively. It is dif cult to estimate the concentration of the cis isomer in the lm because the e value of the n p* transition of the cis isomer is unknown. It is reasonable that a portion of the azobenzene ligands are in the cis conformation because the gel shrinkage during the lm formation process caused by ethanol evaporation leads to a portion of the azobenzene ligands adopting the cis conformation with shorter molecular length. Only upon powerful stimulation (heat) to overcome the force (B200 pN/ azobenzene ligand [Hugel et al., 2002]) involved in the conformational change does the cis isomer change to the trans isomer that has a longer molecular length. 13.4.2.3. Stress Development and Relaxation of Azobenzene-Modi ed Polysilsesquioxane Gels. The dimensional change associated with the trans 2cis isomerization of the azobenzene ligands contained in the polysilsesquioxane gel lms causes the gel network to shrink or expand in response to light stimuli, which involves stress development and relaxation of the lm. Brinker and coworkers used a homemade beam bending setup to observe the stress behavior in response to UV light irradiation. The in-plane stress during alternating UV light exposure and dark exposure is calculated from Stoney s equation as follows: s Es ds2 d Vs df

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Companies like Axiom (www.axiom.com), Rapleaf (www. rapleaf.com), and Unbound Technologies (www. unboundtech.com) are mapping the relationships in a different way. Rather than follow conversations, which is tricky at best, these companies scour the social networking sites and blogs for friends and blogrolls. This information is declarative rather than inferred. I am your friend. I include you in my blogroll to indicate that I think your posts are worth reading. This information is there for the taking it s public. With this connection information, Axiom can match their own database with yours and report back on which of your customers or prospects is linked to which others. You now know how your community is linked. That is, you know which of those in your database make up a sub-community. That s invaluable for sending targeted messages.

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